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2761 items
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Understanding the effect of synthesis and sintering temperature on the functional properties of barium titanate/cobalt ferrite composites
Marija Šuljagić, Aleksandar Kremenović, Ivan Petronijević, Adis Džunuzović, Miljana Mirković, Vladimir Pavlović, Ljubica Anđelković (2023)To investigate the effect of synthesis procedure and sintering temperature on the functional properties of perovskite/spinel ceramics, BaTiO3/CoFe2O4 composites were prepared by thermal decomposition, coprecipitation, and microemulsion method, and sintered at 1150°C and 1300°C. The phase composition and morphology of as-prepared powders as well as sintered ceramics were thoroughly examined by X-ray powder diffraction (XRPD) and scanning electron microscopy (SEM) coupled with electron dispersive spectroscopy (EDS). The dielectric and ferroelectric measurements were performed in detail. Generally, the ...Marija Šuljagić, Aleksandar Kremenović, Ivan Petronijević, Adis Džunuzović, Miljana Mirković, Vladimir Pavlović, Ljubica Anđelković. "Understanding the effect of synthesis and sintering temperature on the functional properties of barium titanate/cobalt ferrite composites" in Science of Sintering (2023). https://doi.org/10.2298/SOS220512013S
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Synthesis and characterization of high-pressure and high-temperature sphene (CaTiSiO5)
Jelena Pantić, Vladimir Urbanovich, Vesna Poharc-Logar, Bojan Jokić, Marija Stojmenović, Aleksandar Kremenović, Branko Matović (2014)Sphene (CaTiSiO5), a calcium titanosilicate ceramic has been prepared from a powder mixture of CaCO3, TiO2 and SiO2 using vibro-milling for homogenization and activation of precursors. During the highpressure and high-temperature synthesis (HPS) process at 4 GPa and 1,200 °C, sphene undergoes into phase transition, from room-temperature phase P21/a to high-temperature phase A2/a. Evidence of that structural phase transition is given in this paper using infrared, Raman spectroscopy and X-ray powder diffraction. Rietveld refinement was employed to get the ...Jelena Pantić, Vladimir Urbanovich, Vesna Poharc-Logar, Bojan Jokić, Marija Stojmenović, Aleksandar Kremenović, Branko Matović. "Synthesis and characterization of high-pressure and high-temperature sphene (CaTiSiO5)" in Physics and Chemistry of Minerals, Springer Science and Business Media LLC (2014). https://doi.org/10.1007/s00269-014-0693-x
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Influence of Post-Synthesis Treatments on the Properties of Brushite/Monetite Powders
Željko Radovanović, Lidija Radovanović, Aleksandar Kremenović, Đorđe Janaćković, Rada Petrović (2022)Dicalcium phosphate (DP) materials, of which brushite and monetite were the most known, have been intensively studied for several decades because of excellent resorptive and osteoconductive properties that can satisfy the requirements needed for various medical applications, such as bone cements, coatings of metallic implants and bone grafts ...Željko Radovanović, Lidija Radovanović, Aleksandar Kremenović, Đorđe Janaćković, Rada Petrović. "Influence of Post-Synthesis Treatments on the Properties of Brushite/Monetite Powders " in Second International Conference on Electron Microscopy of Nanostructures ELMINA 2022, August 22nd–26th, 2022, Belgrade, Serbia, Serbian Academy of Sciences and Arts Knez Mihailova 35, 11000 Belgrade, Serbia (2022)
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Novel cerium and praseodymium doped phosphate tungsten bronzes: Synthesis, characterization, the behavior in the Briggs-Rauscher reaction and photoluminescence properties
Tijana Maksimović, Pavle Tančić, Jelena Maksimović, Dimitrije Mara, Marija Ilić, Rik Van Deun, Ljubinka Joksović, Maja Pagnacco (2023)Due to the interesting and potentially useful properties, phosphate tungsten bronzes are constantly being studied and attract a lot of attention. In the present work, two different metallic elements, belonging to the group of rare-earth metals, cerium and praseodymium, were used as a dopants for phosphate tungsten bronzes. Novel cerium and praseodymium doped phosphate tungsten bronzes were successfully synthesized and further characterized by thermal analyses, Fourier-transform infrared spectroscopy, X-ray powder diffraction, scanning electron microscopy with energy-dispersive X-ray spectrometer and ...Electrical and Electronic Engineering, Atomic and Molecular Physics and Optics, Electronic, Optical and Magnetic Materials, Inorganic Chemistry, Organic Chemistry, Physical and Theoretical Chemistry, SpectroscopyTijana Maksimović, Pavle Tančić, Jelena Maksimović, Dimitrije Mara, Marija Ilić, Rik Van Deun, Ljubinka Joksović, Maja Pagnacco. "Novel cerium and praseodymium doped phosphate tungsten bronzes: Synthesis, characterization, the behavior in the Briggs-Rauscher reaction and photoluminescence properties" in Optical Materials, Elsevier BV (2023). https://doi.org/10.1016/j.optmat.2023.114125
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Mechanical activation and silver supplementation as determinants of the antibacterial activity of titanium dioxide nanoparticles
Ljubica Anđelković, Marija Šuljagić, Vladimir Pavlović, Miljana Mirković, Boško Vrbica, Irena Novaković, Dalibor Stanković, Aleksandar Kremenović, Vuk Uskoković (2024)This study employed a novel synthetic approach involving a modified reverse co-precipitation method utilizing glacial acetic acid to synthesize α-Bi2O3 . X-ray powder diffraction and scanning and transmission electron microscopy analyses revealed the formation of a rod-like α-Bi2O3 microstructure. The prepared material was utilized to modify a glassy carbon paste (GCP) electrode for the development of an electrochemical sensor for acetaminophen (APAP) detection using differential pulse voltammetry (DPV). Cyclic voltammetry studies revealed that the GCP@Bi2O3 electrode exhibited enhanced electrochemical properties compared to the bare ...štapićasta a-Bi2O3 mikrostruktura, reverzna sinteza ko-precipitacije, elektrohemijski senzor, detekcija acetaminofenaLjubica Anđelković, Marija Šuljagić, Vladimir Pavlović, Miljana Mirković, Boško Vrbica, Irena Novaković, Dalibor Stanković, Aleksandar Kremenović, Vuk Uskoković. "Mechanical activation and silver supplementation as determinants of the antibacterial activity of titanium dioxide nanoparticles" in Colloids and Surfaces A: Physicochemical and Engineering Aspects, Elsevier BV (2024). https://doi.org/10.1016/j.colsurfa.2024.133890
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Synthesis and characterization of nanostructured Ca0.9Er0.1MnO3
Tijana B. Vlašković, Bojana Laban, Maja Milošević, Maria Čebela, Vladimir Dodevski, Milena Rosić (2023)Tijana B. Vlašković, Bojana Laban, Maja Milošević, Maria Čebela, Vladimir Dodevski, Milena Rosić. "Synthesis and characterization of nanostructured Ca0.9Er0.1MnO3" in Book of Abstracts Proceedings / 59th Meeting of the Serbian chemical society, Novi Sad, Serbia, June 1-2, 2023, Belgrade : Serbian Chemical Society (2023)
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Preparation, synthesis and characterization of nanometric Ca0.9Er0.1MnO3
Tijana B. Vlašković, Bojana Laban, Maja Milošević, Maria Čebela, Vladimir Dodevski, Milena Rosić (2023)Tijana B. Vlašković, Bojana Laban, Maja Milošević, Maria Čebela, Vladimir Dodevski, Milena Rosić. "Preparation, synthesis and characterization of nanometric Ca0.9Er0.1MnO3" in Programme and Book of abstracts 15th ECerS Conference for Young Scientists in Ceramics, Novi Sad, Serbia October 11-14, 2023 , Novi Sad : Faculty of Technology, University of Novi Sad (2023)
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Synthesis, characterization and photocatalytic examination of Co0.9Ho0.1MoO4 nanopowders
Milena Rosić, Maja Milošević, Maria Čebela, Vladimir Dodevski, Vesna Lojpur, Radomir Ljupković, Aleksandra Zarubica (2023)Milena Rosić, Maja Milošević, Maria Čebela, Vladimir Dodevski, Vesna Lojpur, Radomir Ljupković, Aleksandra Zarubica. "Synthesis, characterization and photocatalytic examination of Co0.9Ho0.1MoO4 nanopowders" in Programme and the book of abstracts 7th Conference of The Serbian Society for Ceramic Materials 7CSCS-2023, June 14-16, 2023 Belgrade, Serbia , Beograd : Institut za multidisciplinarna istraživanja (2023)
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The Fuzzy–AHP Synthesis Model for Energy Security Assessment of the Serbian Natural Gas Sector
Natural gas is used for the production of almost 20% of total energy today. The natural gas security of the Republic of Serbia is an urgent strategic, political and security issue. Serbia is one of the most vulnerable countries in Southeast Europe, because it only has one supply route. This study is a contribution to efforts to better understand the factors affecting energy security through the implementation of a new methodology based on the fuzzy–AHP synthesis model for measuring ...Aleksandar R. Madžarević, Dejan D. Ivezić, Miloš L. Tanasijević, Marija A. Živković. "The Fuzzy–AHP Synthesis Model for Energy Security Assessment of the Serbian Natural Gas Sector" in Symmetry, MDPI AG (2020). https://doi.org/10.3390/sym12060908
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A new copper(II) arsenate, Na2Cu3(AsO3OH)4·4H2O containing discrete [Cu3O12]18− units: Synthesis, crystal structure and magnetic properties
Single crystals of the new disodium tricopper(II) tetrakis(hydrogenarsenate(V)) tetrahydrate, Na2Cu3(AsO3OH)4·4H2O were grown under hydrothermal conditions. The compound was characterized by room-temperature single-crystal X-ray diffraction, SEM-EDS analysis, Raman spectroscopy and magnetic susceptibility measurements. Na2Cu3(AsO3OH)4·4H2O represents a new layered structure-type [space group P21/c, a = 8.7089(17), b = 9.7452(19), c = 9.3353(19) Å, β = 92.63(3)°, V = 791.4(3) Å3, Z = 4]. The layers are normal to [100] and are composed of the isolated Cu3O12 units interconnected by AsO3OH coordination ...Na2Cu3(AsO3OH)4•4H2O, хидротермална синтеза, кристална структура, хидрирани хидрокси-арсенати, магнетна својстваTamara Đorđević, Ljiljana Karanović, Zvonko Jagličić. "A new copper(II) arsenate, Na2Cu3(AsO3OH)4·4H2O containing discrete [Cu3O12]18− units: Synthesis, crystal structure and magnetic properties" in Journal of Solid State Chemistry, Elsevier BV (2018). https://doi.org/10.1016/j.jssc.2018.05.024
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A new polymorph of Ba(AsO3OH): Synthesis, crystal structure and vibrational spectra
Tamara Đorđević, Ljiljana Karanović (2010)A new monoclinic polymorph of Ba(AsO3OH) was synthesized under hydrothermal conditions. It represents a previously unknown structure type. Its crystal structure was determined from a racemic twin using single-crystal X-ray diffraction data collected at 120 and 293 K [space group P21, a=7.2149(14)/7.2370(2), b=7.7028(15)/7.7133(2), c=21.7385(43)/21.8079(5) Å, β=95.95(3)/96.073(1)1, V=1201.6(4)/1210.51(5) Å3, Z=12]. The crystal structure of P21-Ba(AsO3OH) has a layered character and is built up of four types of regularly alternating layers parallel to (0 0 1). Every AsO3OH tetrahedron is chelating to two Ba atoms and ...Ba(AsO3OH), хидротермална синтеза, структурна анализа монокристала, Раманска спектроскопија, инфрацрвена спектроскопија, водоничне везе, хидрогенарсенати земноалкалних металаTamara Đorđević, Ljiljana Karanović. "A new polymorph of Ba(AsO3OH): Synthesis, crystal structure and vibrational spectra" in Journal of Solid State Chemistry, Elsevier BV (2010). https://doi.org/10.1016/j.jssc.2010.09.027
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Ionothermal synthesis and crystal structure of a new organic–inorganic hybrid compound:catena-poly[bis(1-ethyl-3-methylimidazolium) [hepta-μ-bromido-pentacuprate(I)]]
A new organic-inorganic hybrid compound, catena-poly[bis(1-ethyl-3-methylimidazolium) [μ5-bromido-tri-μ3-bromido-tri-μ2-bromido-pentacuprate(I)]], {(C6H11N2)2[Cu5Br7]}n, has been obtained under ionothermal conditions from a reaction mixture containing Ba(OH)2•8H O, Cu(OH)2•2H2O, As2O5 , 1-ethyl-3-methylimidazolium bromide and distilled water. The crystal structure consists of complex [Cu5Br7]2- anions arranged in sinusoidal {[Cu5Br7]2-}n chains running along the a axis, which are surrounded by 1-ethyl-3-methylimidazolium cations. Three of the five unique Br atoms and one of the three Cu(I) atoms occupy special positions with half-occupancy (a mirror plane perpendicular to the b ...кристална структура, органско-неорганско хибридно једињење, бакар(I) бромид, јонотермна синтеза, 1-етил-3-метилимидазолијум бромид, Cu•••Cu интеракцијеLjiljana Karanović, Dejan Poleti, Tamara Đorđević. "Ionothermal synthesis and crystal structure of a new organic–inorganic hybrid compound:catena-poly[bis(1-ethyl-3-methylimidazolium) [hepta-μ-bromido-pentacuprate(I)]]" in Acta Crystallographica Section C Structural Chemistry, International Union of Crystallography (IUCr) (2014). https://doi.org/10.1107/S205322961402172X
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From mixed brookite/anatase TiO2 nanopowder to sodium titanates: Insight into morphology, structure, and photocatalytic performance
Nataša Tomić, Mirjana Grujić-Brojčin, Aleksandar Kremenović, Mirjana Novaković, Vladimir Lazović, Maja Šćepanović (2024)A method to obtain sodium titanate nanoribbons starting from a mixture of brookite and anatase TiO₂ nanopowder is described. As-prepared TiO2 nanopowder with a major brookite phase was used as a precursor in an alkaline hydrothermal approach, where the temperature was kept at 200 °C. The influence of hydrothermal treatment and consequent annealing temperature (T = 500 ) on the crystal structure, phase composition, and morphology of samples were investigated by X-ray powder diffraction (XRPD), Raman and FTIR spectroscopy, ...nanostrukturirani materijali, hemijska sinteza, difrakcija rendgenskih zraka, skenirajuća elektronska mikroskopija, kristalna struktura, katalizaNataša Tomić, Mirjana Grujić-Brojčin, Aleksandar Kremenović, Mirjana Novaković, Vladimir Lazović, Maja Šćepanović. "From mixed brookite/anatase TiO2 nanopowder to sodium titanates: Insight into morphology, structure, and photocatalytic performance" in Ceramics International, Elsevier BV (2024). https://doi.org/10.1016/j.ceramint.2024.10.063
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Water in the Alluaudite Type-Compounds: Synthesis, Crystal Structure and Magnetic Properties of Co3(AsO4)0.5+x(HAsO4)2−x(H2AsO4)0.5+x[(H,□)0.5(H2O,H3O)0.5]2x+
In this study, a new cobalt arsenate belonging to the alluaudite supergroup compounds with the general formula of Co3(AsO4)0.5+x(HAsO4)2−x(H2AsO4)0.5+x[(H, )0.5(H2O,H3O)0.5]2x+ (denoted as CoAsAllu) was synthesized under hydrothermal conditions. Its crystal structure was determined by a room-temperature single-crystal X-ray diffraction analysis: space group C2/c, a = 11.6978(8), b = 12.5713(7), c = 6.7705(5) Å, b = 113.255(5)◦, V = 914.76(11) Å3, Z = 2 for As6H8Co6O25. It represents a new member of alluaudite-like protonated arsenates and the first alluaudite-like phase ...супергрупа алуаудита, арсенати прелазних метала, хидротермална синтеза, кристална структура, хидратисани хидрокси-арсенати, стехиометрија, магнетна својстваTamara Đorđević, Ljiljana Karanović, Marko Jagodič, Zvonko Jagličić. "Water in the Alluaudite Type-Compounds: Synthesis, Crystal Structure and Magnetic Properties of Co3(AsO4)0.5+x(HAsO4)2−x(H2AsO4)0.5+x[(H,□)0.5(H2O,H3O)0.5]2x+" in Minerals, MDPI AG (2021). https://doi.org/10.3390/min11121372
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Развој модела употребног квалитета помоћне механизације на површинским коповима лигнита
Драгица Јагодић Крунић (2021)Тренутно стање помоћне механизације на површинским коповима лигнита је незадовољавајуће узроковано пре свега старошћу и неблаговременом заменом машима услед чега је расположивост недовољна а трошкови експлоатације и одржавања високи. Тренутно стање и захтеви који се постављају пред ове машине указују на неопходност оптимизације процеса управљања помоћном механизацијом. Одређивање оптималног времена замене и преосталих могућности је најодговорнији управљачки задатак који треба да буде заснован на свеобухватном сагледавању економских, техничких и других узрочно последичних веза. Са економског аспекта гледано треба одржавати ...помоћна механизација, употребни квалитет, ефективност, расположивост, сигурност функционисања, ризик, трошкови животног циклуса, фази логика, Монте Карло методаДрагица Јагодић Крунић. Развој модела употребног квалитета помоћне механизације на површинским коповима лигнита, Београд : [Д. Јагодић Крунић], 2021
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Synthesis of MnCo2O4 nanoparticles as modifiers for simultaneous determination of Pb(II) and Cd(II)
The porous spinel oxide nanoparticles, MnCo2O4, were synthesized by citrate gel combustion technique. Morphology, crystallinity and Co/Mn content of modified electrode was characterized and determined by Fourier transform infra-red spectroscopy (FT-IR), scanning electron microscopy (SEM), energy dispersive spectrometry (EDS), X-ray diffraction pattern analysis (XRD), simultaneous thermogravimetry and differential thermal analysis (TG/DTA). Nanoparticles were used for modification of glassy carbon electrode (GCE) and new sensor was applied for simultaneous determination of Pb(II) and Cd(II) ions in water samples with the ...Vesna Antunović, Marija Ilić, Rada Baošić, Dijana Jelić, Aleksandar Lolić. "Synthesis of MnCo2O4 nanoparticles as modifiers for simultaneous determination of Pb(II) and Cd(II)" in PLOS ONE (2019). https://doi.org/10.1371/journal.pone.0210904
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Sinteza i strukturna karakterizacija mikroporoznih arsenata i fosfata
Sabina Z. Kovač (2015-09-28)Predmet rada i istraživanja ove doktorske disertacije su sinteza i strukturnekarakteristike novih kristalnih arsenata i fosfata koji sadrže Mg, K, Ca, Mn, Fe, Co, Ni,Cu, Zn, Sr, Ba i druge katjone. U strukturama arsenata i fosfata, AsO4- i PO4-tetraedrinajčešće se vezuju sa tetraedarski ili oktaedarski koordinisanim katjonima prelaznihmetala formirajući otvorene strukture (slojeve ili 3D mreže) sa širokim opsegomrazličitih topologija. U šupljinama ili porama u obliku povezanih ili nepovezanihkanala, tunela, kaveza i međuslojnog prostora mogu se ugraditi različiti vanmrežni joni(obično ...Sabina Z. Kovač. "Sinteza i strukturna karakterizacija mikroporoznih arsenata i fosfata" in Универзитет у Београду, Универзитет у Београду, Рударско-геолошки факултет (2015-09-28)
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Tl(I) sequestration by pharmacosiderite supergroup arsenates: synthesis, crystal structures and relationships in Tl(I)–M(III)–As(V)–H2O (M = Al, Fe) system
Tamara Đorđević, Tarik Karasalihović, Michael Stöger-Pollach, Ljiljana Karanović. "Tl(I) sequestration by pharmacosiderite supergroup arsenates: synthesis, crystal structures and relationships in Tl(I)–M(III)–As(V)–H2O (M = Al, Fe) system" in Mineralogy and Petrology, Springer Science and Business Media LLC (2023). https://doi.org/10.1007/s00710-023-00823-4
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Solid state synthesis of extra phase-pure Li4Ti5O12 spinel
Фазно чист спинел Li4Ti5O12 са величином честица мањом од 500 nm добијен је реакцијом у чврстом стању из стехиометријске смеше наноанатаса (ТiО2) и Li2CO3 која је претходно активирана механохемијским поступком. Реакција у чврстом стању у потпуности се завршава за само 4 часа на температури од 800 ºC. Уз помоћ XRPD, SEM и TG/DSC анализе испитане су структурне и микроструктурне карактеристике добијеног спинела, механизам реакције између анатаса и Li2CO3, као и термичка стабилност Li4Ti5O12. Реакција започиње разлагањем Li2CO3 на температурама ...дифракција рендгенских зрака, механизам реакције, термичка стабилност, Li4Ti5O12, спинел, фазно чист узоракIvana Veljković, Dejan Poleti, Ljiljana Karanović, Miodrag Zdujić, Goran Branković. "Solid state synthesis of extra phase-pure Li4Ti5O12 spinel" in Science of Sintering, National Library of Serbia (2011). https://doi.org/10.2298/SOS1103343V
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Синтеза, структурне и магнетне особине Ca1-xGdxMnO3 нанопрахова
Milena Rosić (2014-12-05)У оквиру ове докторске тезе, испитиване су оптималне методе за добијањенанопраха – калцијум манганског оксида допираног јонима гадолинијума. Циљистраживања је испитивање одговарајућих прекурсора који су подесни да седобију чисти нано прахови манганита са перовскитском структуром, као имонофазни чврсти раствори са перовскитском структуром. Као подесан методкоришћена је модификована глицин нитратна метода, а од прекурсора нитрати иацетати одговарајућих метала. Модификација глицин нитратне методе се односина делимичну замену нитрата ацетатима, чиме је ублажена бурност реакције.Испитан је различити однос прекурсора, који дају наночестичне ...Milena Rosić. "Синтеза, структурне и магнетне особине Ca1-xGdxMnO3 нанопрахова" in Универзитет у Београду, Универзитет у Београду, Рударско-геолошки факултет (2014-12-05)